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81.
I.Z. Ismagilov R.P. Ekatpure L.T. Tsykoza E.V. Matus E.V. Rebrov M.H.J.M. de Croon M.A. Kerzhentsev J.C. Schouten 《Catalysis Today》2005,105(3-4):516-2
This paper describes the optimization of three processes applied in fabrication of a microstructured reactor for complete oxidation of volatile organic compounds. The first process involves the optimization of the electro discharge machining (EDM) method to produce a set of microchannels with a high length to diameter ratio of 100, with a standard deviation from the average diameter below 0.2%, and with a surface roughness not higher than 2.0 μm. To satisfy these criteria, fabrication of microchannels must be carried out with two machining passes in the Al51st alloy. Then, the effect of several parameters on the anodization current efficiency with respect to oxide formation was studied. The best process conditions to get a 30 μm porous alumina layer in a 0.4 M oxalic acid electrolyte, were found to be a temperature of 1 °C, an anodic current density of 5 mA/cm2, and 23 h oxidation time. At last, the resulting coatings were impregnated with an aqueous solution of copper dichromate followed by drying and calcination at 450 °C to produce active catalysts. The effect of a copper dichromate concentration, number of impregnation cycles (1 or 2), and different after-treatments on catalytic activity and stability in complete oxidation of n-butane were studied. The catalytic activity of the obtained coatings is superior to that of alumina supported pelletized catalysts even at much lower loadings of active metals. 相似文献
82.
Tsung-Kuang Yeh Ming-Han Tsai Mei-Ya Wang Chen-Kuo Weng 《Journal of Applied Electrochemistry》2008,38(11):1495-1500
In the preparation of copper interconnects in the conductor pattern of a printed circuit board (PCB), wet etching processes
are commonly adopted for creating patterns of high-density interconnects. Currently available techniques of immersion and
spray etching could lead to poorly shaped wires due to complex flow fields or the disturbing puddling effect. A modified technique
of arrayed jet-stream etching was developed in this work, aiming at producing well-defined copper interconnects on a PCB in
a significantly shorter time. The results were appealing in that copper interconnects of 35/140 μm (thickness/width) exhibiting
etching factors of greater than 6 were obtained in 20 s, much better than the conventional ones with etching factors of 3
to 5 and etching times of at least 2 min. In addition, uniformly etched copper interconnects with less than 20 μm undercuts
were observed on one etching line. One additional point to note is that no banking agents or inhibitors as commonly seen in
conventional etching techniques were needed in this new processing method. 相似文献
83.
Veysel T. Yilmaz Evrim Senel Canan Kazak 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(3):407-413
The reaction of [Cu(sac)2(H2O)4] · 2H2O with 2-methylpyrazine (mpyz) leads two complexes, concomitant crystallization of a mononuclear complex [Cu(sac)2(mpyz)(H2O)2] (1) and a polymeric complex [Cu(sac)2(μ-mpyz)]n (2). Both complexes have been characterized by elemental analyses, magnetic measurements, FT-IR and ESR, TG-DTA and single-crystal
X-ray diffraction analyses. Single-crystal X-ray analyses show that complex 1 consists of discrete molecules in which the copper(II) ions exhibits a square-pyramidal coordination geometry. The individual
molecules of 1 are connected into a hydrogen-bonded chain structure, which is further assembled to form a three-dimensional network by π–π stacking interactions.
Complex 2 is an 1D coordination polymer in which copper(II) centers are bridged by the mpyz ligand. The chains are further assembled
to form two-dimensional frameworks by π–π and C–H···π stacking interactions. 相似文献
84.
深基坑工程长近百米,周边环境复杂,施工作业条件差,结合工程设计留设的后浇带,采用适合的支护结构体系、止水帷幕技术、土方开挖方法,加强施工监测,着力于减少对周边环境的不利影响,为类似条件的深基坑工程的施工提供了有益的经验。 相似文献
85.
成品油储罐内的腐蚀及防护 总被引:1,自引:0,他引:1
对成品油储罐内各部位腐蚀情况进行了介绍,说明了产生腐蚀的原因和腐蚀机理。介绍了油罐内防护技术,采用节点加固,降低边缘应力,可减缓油罐金属腐蚀速度;对选用油罐内防腐涂料的原则进行了阐述。 相似文献
86.
招远金矿集中区是我国最大的金矿集中区,区内金矿床在时间和空间上的分布规律十分明显。该区矿化类型主要有石英脉型、蚀变岩型及二者之间的过渡类型,其在空间上的分布规律为综合信息找矿及矿床定位预测提供地质信息,并可作为进一步的找矿标志。 相似文献
87.
88.
89.
利用AES、WDS和x-射线衍射等方法,研究了杜美丝表面层、铁镍芯与覆铜层界面的微观结构与特性。结果表明:良好的表面层应由Cu2O和非晶态的硼砂构成;玻璃与杜美丝的润湿性决定于表面层的净化程度和构成及加热条件。 相似文献
90.